X met 5100 руководство по эксплуатации

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  X-MET5000 /X-MET5100

  Oxford Instruments Industrial Analysis

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  Ver 2

  October 2009

  SW version 1.1 / 2.0 / 3.0

  Quick Start Guide

  X-MET5000 / X-MET5100

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  X-MET Radiation Safety

  Please read the Users Manual carefully before operating the

  X-MET analyzer. This quick start manual is a summary of the

  actual users manual.

  Radiation safety and user training is required before
  operating

  the analyzer.

  Follow all the safety instructions in Users Manual, such as:

  Do not let any person closer than one meter from the

  primary X-ray beam

  Never point the radiation beam towards yourself or anyone

  else.

  Ensure that the analyzer is in touch with the sample all the

  time while measuring.

  Keep the instrument at a right-angle (90) against the

  sample to minimize scattering radiation

  While measuring small samples, use bench top stand,

  background plate or radiation shield to minimize the

  scattering radiation.

  Protect the unit with password to prevent unauthorized use.

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  Radiation Protection

  — Examples of potential misuse

  Do not let any person closer than

  one meter from the primary X-ray

  beam

  Do not point the analyzer at any

  body part

  Do not measure against any body

  part

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  Do not use fingers or other body

  parts to block the IR sensor. Use

  safety shield when measuring

  small samples.

  Keep the instrument in touch with

  the sample during the whole

  measurement.

  Keep the instrument at correct

  angle (90) against the sample to

  minimize scattering radiation.

  When measuring repeatedly low

  density samples such as plastic,

  wood, paper, soil or minerals

  safety shield should be used.

  Radiation Protection

  — Examples of potential misuse

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  About the battery

  The battery is located inside the handle of the

  X-MET unit. To replace the battery, push the switch and pull

  the battery out of the handle.

  Each fully charged battery gives

  approximately 4 — 5 hours of operating time.

  Change the battery when battery indicator on

  the PDA screen turns to red (only one bar left).

  There is also a battery indicator on the side of

  the battery. Push and hold the button to check

  battery status. If only one led will ignite, charge

  the battery before starting the measurements.

  Recharging the battery

  Before removing the battery, exit X-MET

  program and turn off the analyzer. You can

  also charge without disconnecting it from the

  X-MET.

  Attach the battery to the charger. When the

  Power LED is green, charger is operational.

  Blinking green Charger LED indicates that the

  battery is charging.

  When the battery is fully charged, the Charger

  LED turns to green.

  Blinking red Charger LED indicates that either

  the battery or the charger is faulty.

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  Basic Use of the Analyzer

  Indicator lightsThe green light indicates that the power is on.
  The

  green light turns to yellow when IR proximity

  sensor sees sample in front of the analyzer nose.

  When the red light is lit, x-rays are being

  generated. There are three x-ray warning lights:

  one on each side of the analyzer nose and one on

  the back below PDA.

  IR proximity sensor

  To start the measurement the IR sensor must be

  covered by the sample. This will prevent

  accidental exposure to radiation. The green status

  light will turn to orange when sample covers the

  IR sensor.

  Disconnecting PDA

  Before disconnecting PDA exit X-MET programand turn off the unit
  from main power switch. To

  disconnect PDA first remove the rubber frame and

  possible rain cover. Then slide out PDA carefully.

  Be careful and do not use force when connecting

  PDA back to X-MET to prevent damage to the

  connectors.

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  Measuring with optional light travel stand

  1

  2

  3

  4

  5

  ChargerConnect cables 3 and 5 directly to the charger,

  then connect mains cable to AC outlet.

  Light travel stand (optional accessory).

  Remove the PDA and place X-MET firmly to the stand.

  Data/power cable Connect one end to the charger1 and

  other end to the X-MET battery

  PDA chargerConnect one end to the mains outlet

  and the other end to the small connector in cable 5.

  PDA connection cable Connect one end to the charger

  1 and other end to the PDA. The third connector (USB) will

  not be used.

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  Switching the analyzer on and off

  To switch on analyzer:

  1. Push the power button until the green standby-light is lit.
  Notice that

  the standby light turns to yellow when the proximity sensor
  detects a

  sample in front of the analyzer nose.

  2. Push the calendar button and the X-MET software will start.
  If the

  software fails to initialize tap the Windows flag icon in top
  left cornerof the PDA screen and select X-MET

  To switch off analyzer:

  Push and hold the power button until you see that the
  progress-bar

  on PDA screen is full. PDA will switch itself off
  automatically.

  Power button

  Calendar button

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  Starting up the Analyzer

  Start up the Analyzer by pushing the power buttonuntil the
  status-light turn to green.

  Start the X-MET operating software by pressing

  the PDA Calendar button or:

  Push the power key in top right corner of the

  PDA.

  Tap the START icon on the top left corner of

  the PDA screen. (Figure 1)

  Choose X-MET program from the menu.

  X-MET start up screen appears.

  Tap logon when the screen with warning sign

  appears. If your unit is protected with password,

  you must give it in the following screen. You can

  change the password settings in Settings ->

  User Setup.

  The unit will automatically go to locked mode if it

  havent been used for 5 minutes. To continue

  measuring, password is required.

  The measurement screen will appear. In this

  mode the analyzer is ready to use. Tapping the

  screen will open the main menu (figure 4).

  1

  2

  3

  4

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  Main menu Status bar

  explanation of the symbols

  1 2 3 4 5 6

  1. Active Calibration method

  2. If Result Format is activated, it is shown here

  3. Log file is activated when the notepad symbol is shown.

  4. This figure shows the current user level. Two human
  figures

  mean normal user, one human figure means supervisor and

  tool symbol means service level. The user level can be

  changed in settings -> user setup menu.The yellow background
  indicates that the proximity sensor

  detects a sample in front of the analyzer nose and the unit
  is

  ready to measure.

  5. The lightning sign sybolizes that instrument is in mains

  connection.

  6. Battery indicator shows the current charge status of the
  battery.

  When only one red bar is left, it is recommended to shut
  down

  the instruments and change the battery as soon as possible.

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  Selecting the Method

  Screening Method

  (Alloy mode / RoHS mode etc.)

  Methods which are named as mode

  are screening methods. Screening

  method detects automatically thesample type and selects the
  correct

  Empirical or FP method to calculate

  analysis result.

  Empirical Methods (Copper, Titanium etc.)

  Empirical calibration method, which is

  specific for certain sample type or alloy

  group. Empirical calibration works

  properly only with the specific sampletype it is calibrated.

  FP Methods (Alloy_fp, Plastic_fp etc)

  General standardless calibration

  method, which works for wide range of

  materials, like metal alloys or plastics.

  The calibration methods in X-MET are customer and application
  specific so it is

  possible that your analyzer does not have all the methods listed
  below. Proper

  method is chosen from Select Method -menu before starting the
  measurement. Someof the methods are visible only in Supervisor User
  level. In most applications

  Screening method should be used.

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  To change the measurement time, choose Set

  Measurement Time from main menu.

  When the measurement time is set to 0, the

  measurement can be stopped any time by

  releasing the trigger. The results will beconstantly updated on
  the result screen during

  the measurement.

  When value is given (other than 0) for

  measurement time, the measurement will stop

  automatically when the time is elapsed.

  For metal alloys, the typical measurement

  time is 2-20 seconds, depending on thedesired accuracy. Soil and
  plastic samples

  usually require at least 60 seconds

  measurement time for accurate results.

  Setting the measurement time

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  Name the sample before starting the

  measurement.

  To name the sample, choose Name

  Sample from the main menu.

  The sample name (max. 20 characters) will

  be saved in log file, which can be defined in

  Output Settings section.

  Pre-defined sample name can be selected

  from drop down menu. 20 previous sample

  names can be found from the list.

  If space and number are placed after the

  sample name, the program will start to index

  the results automatically. (e.g. Test 1, Test 2,Test 3.
  etc.)

  Maximum 80 characters of additional

  information can be added on Additional

  Information field. The information will also

  be saved in the log file.

  Up to 8 additional information fields can be

  added.

  The optional barcode scanne save the

  barcode information in either name or

  additional information field.

  Naming the Sample

  1

  2

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  The analysis results can be stored

  automatically to PDA main memory or

  memory card.

  Analysis results are saved to LOG file,

  which is a text file, that can be opened

  with almost any text editor (e.g. Microsoft

  Excel, Notepad or optional Oxford

  Instruments Report Generator software).

  When LOG file option is activated, the file

  name and all the results will be saved in

  this file, until the file name will be changed.

  Sample spectra can be automatically

  saved by activating the Spectra directory

  option and defining folder for spectra files.

  This must be done before measuring the

  sample.

  Separate average log file is for averageresults. This log file
  will not include

  individual results but only averages.

  Average will also saved normal log file

  after the individual results.

  GPS log file will create a separate file

  including GPS coordinates and the

  analysis results. This file (.kml) can be

  opened in a map program (e.g. Google

  Earth)

  Easiest way to transfer LOG file to the

  external PC is to use memory card and

  memory card reader which are included

  with the X-MET5000 instrument.

  Output settings

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  Result Screens

  Information which is displayed on result screen

  depend on various user interface settings and used

  calibration method:

  1 Default Result Screen

  Analysis results in % or ppm

  Optional standard deviation (STD) display

  Grade information, grade limits shown on the right.

  Hign and low alert colors are user defineable.

  2 Average Result

  When Average Mode is activated from the Settings

  menu, average can be calculated to 2-50

  measurement results.

  (ReferX-MET5000 Users Manual for more

  information)

  3 Result Format -function

  When customer or application specific Result Format

  is activated from the Main Menu, color coded alarms

  and messages can be displayed for fast decision

  making. (ReferX-MET5000 Users manual for more

  information).

  1

  2

  3

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  Select appropriate method and measurement time.

  Place the measurement window in direct angle against the
  sample.

  Make sure that the sample covers the IR proximity sensor,
  otherwise

  the measurement will not start.

  Keep the trigger pulled during the whole measurement time.

  If the measurement do not start, center the measurement

  window and pull the trigger again.

  In Timed Assay mode (see Users Manual) press and release

  the trigger to start measurement. Measurement can be

  stopped any time by quickly pressing and releasing the
  trigger

  again.

  Measuring the samples

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  Analyzing Metal Samples with X-MET

  For metal alloys, the typical measurement time is 2-20 seconds,
  depending on

  the desired accuracy. If necessary, check that the standard
  deviation (STD) is

  adequate small.

  Make sure that the sample is in the middle of the measurement
  window.

  Cover the whole window with the sample when possible.

  When measuring small samples, use longer measuring time than
  usual.

  Pay attention to the possible coating of the sample. The
  penetration of the

  radiation is typically less than 0.5 mm.

  Rusty / unclean or painted surface may distort the analysis
  results. Clean the

  surface before analyzing.

  Ensure that the measurement window is clean. Metal dust in the
  window

  might have a significant effect on the results.

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  Analyzing plastic, soil and other low density samples

  with X-MET

  For plastics and soil samples it is recommended to use at least
  60 secondmeasurement time to ensure accurate results. Indicative
  screening resultscan be obtained with shorter measurement times.
  Timed Assaymode isrecommended in long measurement times, see Users
  manual for moreinformation.

  Ensure that the sample covers the whole measurement window. In
  casethat sample is not uniform, notice that analysis result is
  average of themeasurement spot. It is recommended to use small
  sample cover,bench-top stand or background plate while analyzing
  plastic or other lowdensity samples.

  It is recommended that the plastic samples should be at least 3
  mm thickto reach the optimal accuracy. It is possible to measure
  thinner samples

  (1 mm and up) for indicative screening analysis. It is
  recommended to pileup thinner samples if possible.

  Make sure that both the measurement window and the sample are
  clean.Dirt might have a significant effect on the analysis results.
  Themeasurement window can be cleaned with small soft brush, cloth
  or bygently blowing the dirt away with pressurized air

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  X-MET5000 /X-MET5100

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  Analyzing light elements with X-MET5100

  Light element (Mg, Al, Si, P, S) analysis is much more sensitive
  to sample

  preparation and conditions than heavier elements.

  The following actions ensures quality analysis on light
  elements:

  The measurement window must be clean and intact When measuring
  soil or mining samples the sample must be dry, ground to

  small particle size and homogenized

  Sample cup and thin film (e.g. 4 m Prolene) must be used.
  Plastic sample

  bag is too thick and will block the weak signal coming from
  light elements.

  Typical sample bag will block up to 97 % of incoming aluminum
  signal!

  Metal samples must have clean and even surface. Jagged and
  dirty

  surfaces will cause error on the results.

  Use long enough measurement time (minimum 60 seconds)

  Error in l ight element analysis wi l l af fect also th e heavy
  element resul ts.

  Therefore i t is cr i t ical to p repare the samp le
  properly.

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  X-MET5000 /X-MET5100

  1/19

  2

  2009

  SW 1.1 / 2.0 / 3.0

  X-MET5000 / X-MET5100

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  X-MET5000 /X-MET5100

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  X-MET

  X-MET

  X

  (90)

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  X-MET5000 /X-MET5100

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  —

  X

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  X-MET5000 /X-MET5100

  4/19

  (90)

  —

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  X-MET5000 /X-MET5100

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  X-MET

  4 — 5

  PDA

  LED

  X-METX-MET

  LED

  LED

  LED

  LED

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  X-MET5000 /X-MET5100

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  x x

  PDA

  PDA PDAX-MET

  PDA

  PDA PDAX-MET

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  X-MET5000 /X-MET5100

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  1

  2

  3

  4

  5

  3 5 AC

  PDAX-MET

  /1X-MET

  PDA5

  PDA1 PDA (USB)

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  X-MET5000 /X-MET5100

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  1.

  2. X-MET

  PDAWindows

  X-MET

  PDA

  PDA

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  X-MET5000 /X-MET5100

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  1

  2

  3

  4

  PDAX-MET

  PDA

  PDA

  1

  X-METX-MET

  ->

  5

  4

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  X-MET5000 /X-MET5100

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  1 2 3 4 5 6

  1.

  2.

  3.

  4.

  ->

  5.

  6.

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  X-MET5000 /X-MET5100

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  X-MET

  Alloy mode / RoHS mode mode

  FP

  FPAlloy_fpPlastic_fp

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  X-MET5000 /X-MET5100

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  0

  0

  2-20

  60

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  X-MET5000 /X-MET5100

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  1

  2

  20

  20

  Test 1Test 2Test 3

  80

  8

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  X-MET5000 /X-MET5100

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  PDA

  Microsoft Excel

  Notepad Oxford

  Instrument)

  PC

  X-MET5000

  GPS GPS

  (.kml)

  Google Earth

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  X-MET5000 /X-MET5100

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  1

  2

  3

  1 % ppm

  (STD)

  2 2-50

  X-MET5000

  3 —

  X-MET

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  X-MET5000 /X-MET5100

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  X-MET5000 /X-MET5100

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  X-MET

  2-20

  (STD)

  0.5 mm

  /

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  X-MET5000 /X-MET5100

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  X-MET

  60

  3 mm

  1 mm

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  X-MET5000 /X-MET5100

  X-MET5100

  4

  97 %

  60

Рентген-флуоресцентный анализатор металлов X-MET 5100

Снят с производства

Области применения рентген-флуоресцентного анализатора металлов X-MET 5100: портативный многоцелевой рентген-флуоресцентный анализатор нового поколения с SDD-детектором (кремниевый дрейфовый детектор) и мощной рентгеновской трубкой 45кВ предназначен для анализа химического состава металлов (в том числе, легких вроде и Mg, Al и Si ) и сплавов без применения гелиевых контейнеров или вакуумного насоса, а также оптико-эмиссионных методов. Прибор имеет функцию усреднения эмпирической калибровки, что дает возможность проводить анализ металлов всего за 1 секунду. Основными областями применения анализатора являются подтверждение марки стали, сортировка лома и деталей аэрокосмической индустрии, определение опасных элементов в игрушках, загрязняющих примесей в почве и малые концентрации в руде. Анализатор металлов долговечен, имеет прочный корпус с влаго- и пылезащитой (стандарт IP54 — NEMA 3), способен выдерживать тяжелые условия работы. X-MET 5100 имеет несколько модификаций, предназначенных для конкретных задач контроля: XMET 5100 ALLOY, X-MET 5100 RESTRICTED, XMET 5100 MULTIPURPOSE, XMET 5100 MINING, XMET 5100 SOIL.

Отличительные особенности рентген-флуоресцентного анализатора металлов:

• Оснащенность анализатора кремниевым дрейфовым детектором, мощной рентгеновской трубкой позволяет проводить измерения за 1 секунду
• Возможность анализа большинства металлов (в том числе, и легких) и сплавов
• Отказ от применения гелиевых контейнеров, вакуумного насоса, оптико-эмиссионных методов
• Наличие функции усреднения эмпирической калибровки
• Возможность контроля не только металлов, но и содержания опасных соединений в игрушках и других изделиях, имеющих высокие требования к химическому составу
• Определение загрязняющих почву примесей и содержания металлов в руде
• Оснащенность гибким программным обеспечением
• Оснащенность прочным корпусом с защитой от грязи и воды
• Наличие нескольких модификаций, предназначенных для решения конкретных производственных задач
• Наличие яркого высококонтрастного сенсорного дисплея
• Совместимость с операционными системами Windows
• Наличие мультиязыкового пользовательского интерфейса (русификация имеется)
• Возможность перенесения полученных данных на ПК посредством подключения накопительной карты памяти к ПК или через беспроводную связь (поддерживает режимы передачи данных Wi-fi, Bluetooth)
• Функция «Timed Assay» для получения длительного измерения единичным нажатием триггера

Комплект поставки

• Анализатор металлов
• Заводское свидетельство
• Транспортировочная сумка

Сопроводительная документация при поставке X-MET 5100:

Прибор поставляется в модификации:

• XMET 5100 ALLOY, предназначенный для анализа металлов и сплавов (базовый комплект включает в себя стандартную библиотеку сплавов, в том числе, алюминиевые и магниевые)
• X-MET 5100 RESTRICTED, предназначенный для анализа опасных и тяжелых элементов в пластике и металлах
• XMET 5100 MULTIPURPOSE, предназначенный для металлов и сплавов, определения опасных и тяжелых элементов в пластике и металлах
• XMET 5100 MINING, используется для анализа руд и горных выработок
• XMET 5100 SOIL, предназначен для анализа почв

Дополнительная комплектация прибора:

• Мобильный стенд для контроля и анализа небольших объектов
• Стационарный настольный лабораторный стенд
• Кобура для крепления прибора на поясе
• Портативный КПК
• Портативный принтер для распечатки результатов анализа
• Транспортировочный кейс для перевозки и хранения прибора
• Кюветы для сыпучих проб
• Майларовая пленка для кювет

Внимание! Производитель оставляет за собой право изменить комплект поставки.

Сертификаты

Все модификации анализатора металлов и сплавов X-MET 5100 сертифицированы в соответствии системам CE и cCSAu.

Дополнительно

Отличный современный прибор X-MET 5100 осуществляет экспресс-анализ металлов, руды, пластиков, порошков и других материалов. Это наиболее подходящий вариант, если нужна эргономичность и хорошая производительность. В перечень исследуемых элементов входят все от Mg до U.

X-MET 5100, к тому же, достаточно прост в использовании и легко обслуживается. Применяется в России и за рубежом в сферах металлургии, машиностроении, научно-исследовательских учреждениях, нефтехимии, в геологической разведке и на горных предприятиях.

Прибор X-MET 5100 составляет серьезную конкуренцию для аппаратов своего класса и ценового уровня. Он выделяется большим перечнем различных аналитических функций, высокой точностью, надежностью и возможностью оптимизироваться под выполнение очень сложных задач.

Аппарат оснащен специальным датчиком высокого разрешения из кремния и долговечной рентгеновской трубкой достаточно большой мощности. При всем этом, измеритель потребляет сравнительно мало энергии и способен функционировать до двенадцати часов без перерывов. Прибор обладает хорошей скоростью, одно измерение занимает не более двух секунд, а для анализа сплава достаточно пяти.

К набору возможностей аппарата необходимо обязательно добавить исследование изделий практически любых габаритов, консистенции и формы, самостоятельную корректировку уровня концентраций при диагностики малых и образцов легких элементов без продувки с помощью гелия. А также функцию рекалибровки по единственной точке, способностью регулировать размеры областей исследования при помощи специального преобразователя.

Габариты прибора: 90х300х270 мм, вес: 1.7 кг.

Многофункциональный, универсальный, мощный аппарат X-MET 5100 придется по вкусу многим специалистам.

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